X-ray Crystallographic Facility

Print out an X-RAY REQUEST FORM in pdf format.

 

The X-ray Crystallographic Facility of the Department of Chemistry conducts X-ray structure analysis of small-molecule organic or inorganic single crystals submitted primarily by the department. As an extension service, the facility also accepts sample submissions from other departments of the university, and from outside of the university campus.

 

Equipment:

 

The equipment available for X-ray Diffraction experiment include:

 

- Computer-controlled Nonius KappaCCD System

- Oxford Cryostream Variable Temperature Apparatus

- Computers for structure solution and refinement

- On-line searching facility for crystallographic (CCDC) through Marriott Library

 

Services:

 

The laboratory offers a wide range of services including:

 

-         Advice on crystallization of diffraction quality crystals

-         Mounting of crystals, include air, moisture and temperature sensitive samples

-         Determination of crystal system, space group and unit cell parameters

-         Accurate data collection at room or low temperature

-         Data reduction and absorption correction

-         Structure solution and refinement

-         Preparation of high quality molecular plots

-         Detailed report with tables of coordinates and molecular geometry

-         On-line searching facility for crystallographic (CCDC) through Marriott Library

 

Resources:

-         How to Grow Crystals

-         Crystallography 101 (Intro.)

-         All about SHELXL

-         Cambridge Structural Database (CCDC)

 

Please Contact:

 

Dr. Atta M. Arif

Department of Chemistry

University of Utah

315 S. 1400 E. rm 1170

Salt Lake City, UT 841120850

TEL:(801) 581-5320

mailto:arif@chemistry.utah.edu